Yuav ua li cas los hloov cov reagent ntawm ib txoj lw noo noo analyzer
Thaum siv cov khoom ntsuas dej noo thiab tsis tuaj yeem siv cov electrolyte, nws yog ib qho tsim nyog yuav tsum tau hloov cov reagent ntawm cov kab ya raws cov tshuaj ntsuam xyuas. Peb tuaj yeem ua haujlwm zoo dua li cas thiab hloov cov reagent ntawm cov kab ya raws cov tshuaj ntsuam xyuas? Hauv qab no, Jilin Haimai Technology yuav qhia txog yuav ua li cas los hloov cov reagent ntawm cov kab ya raws cov ntsuas dej
1. Npaj ib daim ntawv lim kom huv si, tshem tawm ob lub tshuab ziab khaub ncaws ntawm lub tshuab electrolytic thiab muab tso rau ntawm daim ntawv lim; Tshem tawm cov electrolytic electrode, ncuav tawm cov electrolyte nyob rau hauv lub cathode chamber (electrolytic electrode), thiab maj mam ncuav tawm cov electrolyte nyob rau hauv lub anode chamber (electrolytic cell lub raj mis) (ceev faj tsis txhob ncuav tawm lub stirrer)
Feem ntau, nws tsis tsim nyog los ntxuav cov electrolytic cell. Tom qab kis kab mob, nws yuav tsum tau ua raws li nruj me ntsis raws li (3) kev ntxuav
3. Kev tu: Electrolytic cell fwj, cov raj kom qhuav, cov ntsaws ntsaws ntsaws ruaj ruaj, thiab ntsuas electrodes tuaj yeem ntxuav nrog cov tshuaj methanol lossis lwm cov kuab tshuaj anhydrous, thiab yog tias tsim nyog, lawv tuaj yeem ntxuav nrog dej; Lub cathode chamber (electrolytic electrode) yuav tsum tsis txhob muab ntxuav nrog dej kom ntau li ntau tau. Thaum ntxuav nrog dej, nws yuav tsum tau qhuav kom zoo. Tom qab ntxuav, nws yuav tsum tau qhuav hauv qhov cub ntawm 60 degrees Celsius rau 4 teev, thiab tom qab ntawd txias hauv qhov cub. Nco tseg: ob lub plugs, xov hlau, thiab roj hmab hoses yuav tsum tsis txhob kov cov tshuaj ntxuav thaum ntxuav.
4. Thov ib txheej ntawm lub tshuab nqus tsev roj sib npaug rau qhov sib tsoo ntawm qhov ntsuas electrode, ob lub tshuab ziab khaub ncaws, kev txhaj tshuaj, thiab qhov chaw nres nkoj sealing, thiab nruab rau hauv txoj haujlwm sib thooj. Maj mam tig nws kom muaj kev sib khi zoo. Txhaj kwv yees li 100-120 milliliters ntawm electrolyte rau hauv qhov tsis zoo thiab qhov zoo ntawm cov khoom ntsuas dej noo siv lub funnel los tswj cov kua dej tib yam hauv cov chav tsis zoo thiab zoo. Cov qib kua yuav tsum ncav cuag lub cim hauv qab ntawm lub cell electrolytic. Tom qab ntawd, nruab lub sealing ntsaws thiab lub raj kom qhuav, thiab maj mam tig lawv kom ntseeg tau tias lub foob zoo.
5. Ntxig lub ntsuas hluav taws xob ntsaws ntawm lub xov tooj hluav taws xob rau hauv lub ntsuas hluav taws xob ntawm tus tswv tsev, thiab ntxig cov hluav taws xob electrode ntsaws rau hauv lub qhov hluav taws xob electrolytic ntawm tus tswv tsev. Co lub pas dej ua ke ob peb zaug, qhib lub tshuab hluav taws xob thiab nplawm cov yuam sij, thiab yog tias nws nyob rau hauv lub xeev ntawm iodine ntau dhau, siv 50 μ 1. Txhaj cov dej ntshiab uas tsim nyog rau hauv lub xov tooj ntawm tes (cov koob yuav tsum tau muab tso rau hauv lub cev. kua nto) siv cov tshuaj txhaj, thiab saib cov xim ntawm cov electrolyte txhua lub sijhawm kom txog thaum pib suav. Tig tawm lub nplawm thiab sib npaug co lub xov tooj ntawm tes electrolytic kom tag nrho cov dej noo thiab electrolyte hauv huab cua hauv lub cell. Tom qab ntawd tig rau lub nplawm thiab tso cai rau lub ntsuas kom ncav cuag qhov kawg ntawm qhov kawg, thiab tom qab ntawd txuas ntxiv nrog cov qauv txhaj tshuaj.
6. Cov xim cia ntawm cov electrolyte yog xim av liab lossis xim av xim av. Cov xim yog lub teeb daj thaum siv ib txwm siv.
7. Kev ua tsis tiav ntawm electrolyte: Yog tias muaj ob ntawm peb yam hauv qab no, nws yuav ua tsis tiav. (1) Siv cov electrolyte tsawg kawg ib hlis; (2) Cov xim ntawm cov electrolyte darkens (nyob rau hauv tsis yog iodine xeev); (3) Cov txheej txheem electrolysis nyuaj kom ncav cuag qhov kawg [tom qab rov ua dua lub xov tooj ntawm tes electrolysis ob peb zaug raws li qib 5].
8. Thaum nws yog ib qho nyuaj mus txog qhov kawg thaum siv vim yog ib puag ncig cov av noo, huab cua kub, nquag sampling, leakage ntawm silicone ncoo ntawm qhov chaw txhaj tshuaj, los yog nyuaj rau dissolving cov qauv, yooj yim co lub electrolytic cell tusyees raws li ( 5).
9. Ceev faj: Thaum hloov cov tshuaj reagents, ceev faj tsis txhob nqus los yog kov cov reagents nrog koj txhais tes. Yog hais tias nyob rau hauv kev sib cuag nrog cov reagents, yaug lawv kom huv si nrog dej. Vim muaj cov ntxhiab tsw zoo thiab cov tshuaj lom ntawm cov reagent, qhov cua hauv chav kuaj yuav tsum zoo.
