Debugging ntawm ib tug kab ya raws analyzer
Micro noo noo analyzer, tseem hu ua Karl Fischer moisturizing analyzer, suav nrog cov ntsuas dej noo, ntsuas dej noo, ntsuas dej noo, ntsuas ntsuas dej, thiab ntsuas dej noo. Nws yog tsuas yog siv rau kev tshawb nrhiav cov qauv nrog cov ntsiab lus dej tsawg, thiab tau txhim kho nyob rau hauv xyoo tas los no, zoo heev txhim kho qhov tseeb thiab nthuav dav qhov ntsuas. WS-3 tsis siv neeg ya raws ntsuas ntsuas yog tsim nyog rau kev txiav txim siab ntawm cov kab ya raws hauv cov roj rwb thaiv tsev ntawm cov roj av thiab cov khoom siv tshuaj, kab roj hluav taws xob khoom siv.
Cov txheej txheem electrolytic cell
Maj mam co lub electrolytic cell ntawm tus kab mob moisturizing ob peb zaug kom tag nrho nqus cov dej nyob rau hauv lub puab phab ntsa ntawm lub cell lub raj mis los ntawm cov electrolyte. Tom qab ntawd, muab cov xov tooj hluav taws xob tso rau hauv lub hnab ntim khoom, tig rau ntawm qhov sib tw nplawm, kho qhov nrawm nrawm, thiab tsim ib qho me me vortex ntawm cov kua dej; Ntxig lub ntsuas electrode plug thiab electrolytic electrode plug rau hauv lub qhov (socket) ntawm tus tswv tsev thiab xyuas kom muaj kev sib cuag zoo. Qhib lub tshuab hluav taws xob electrolytic. Kev piav qhia: Nyob rau hauv lub xeev ntawm iodine ntau dhau, lub teeb ntsuab ntawm qhov ntsuas ntsuas lub teeb qhia lub teeb thiab lub teeb pom kev electrolysis tau muab tua tag nrho, tsuas yog ib lub teeb liab tau taws sib cais, thiab cov duab digital tsis suav.
Kho qhov sib npaug ntawm cov electrolyte
Yog hais tias lub cell electrolytic tseem nyob rau hauv ib tug sib sib zog nqus iodine tshaj lub xeev, siv ib tug 50ul micro sampler extract 10ul ntawm distilled dej txhua lub sij hawm, so lub koob nrog lim ntawv, nias lub khawm pib, thiab txhaj ntau zaus hauv qab cov kua theem ntawm electrolytic. cell los ntawm lub qhov nyob rau hauv nruab nrab ntawm qhov txhaj tshuaj cock. Saib xyuas cov xim hloov ntawm cov tshuaj electrolytic txhua lub sijhawm kom txog thaum lub electrolyte tig daj, thiab lub teeb ntsuab ntawm qhov ntsuas teeb liab thiab lub teeb liab electrolytic qhia tias lub txee pib suav. (Thaum siv cov electrolyte tshiab thiab lub raj mis qhuav, kwv yees li ntawm 30-50ul dej yuav tsum tau txhaj.) Tos kom suav nres, ces nres. Nqa cov electrolytic cell thiab maj mam co nws ob peb zaug kom nqus cov dej ntawm sab hauv ntawm lub raj mis dua. Tom qab lub tswb nrov kawg, calibration tuaj yeem ua tiav. (Lub sijhawm hloov tshiab electrolyte yuav tsis ruaj khov heev thaum lub sijhawm no, kwv yees li 2-3 ul ntawm cov dej distilled tuaj yeem raug txhaj kom suav txij li 2000 txog 3000 ug, uas yooj yim dua rau kev ruaj ntseg sai dua.)
Calibration ntawm kab ya raws ntsuas ntsuas
Tom qab cov electrolyte stabilizes, siv ib tug {{0}}.5ul micro injector rho tawm 0.3ul ntawm distilled dej, so lub koob nrog lim ntawv, nias lub pob pib ib zaug, thiab txhaj rau hauv qab no qib kua. Lub ntsuas pib suav thiab mus txog qhov kawg, tso tawm 300 ± 30ug dej. Calibrate tsis tu ncua 2-3 zaug, thiab cov nqi suav yog nyob rau hauv qhov xav tau ntau yam, qhia tias ntsuas qhov tseeb. (Ceeb Toom: Qhov yuam kev ntawm qhov ntsuas dej nrawm nws tus kheej tsis ntau dua ± 0.3 feem pua, tab sis xav tias micro injector muaj peev xwm yuam kev ntawm ± 5 feem pua thiab tib neeg kev ua haujlwm yuam kev, calibration nrog dej distilled (100 feem pua) tau tso cai rau muaj qhov yuam kev hauv ± 10 feem pua.)
